ductile iron
   To Promote the production and application of ductile iron castings Issue 1, 2001   

Ductile Iron Answers the Pipe Maker's Dream
by: Sam F. Carter, Consultant, Retired from ACIPCO

In the forty some years since the invention of Ductile Iron, virtually every manufacturer of pressure pipe has switched from gray iron to this superior metal. Why? Because Ductile Iron's exceptional characteristics enabled improved performance with a reduction in thickness and weight.

Widespread evaluation of Ductile Iron in the 1950s demonstrated its superior strength and impact toughness, prompting more producers to switch from gray iron. By the mid 1970s, all major producers of iron water main pipe had converted entirely to Ductile Iron.

Small diameter pipe of the American Cast Iron Pipe Company with 6 machines centrifigally casting Ductile Iron pipe of 4 to 16 inch diameter in 20 foot length.

The United States currently sees approximately 1 1/4 million tons of Ductile Iron pipe produced annually. And an estimated 1 1/2 million miles of pipe have already been installed to distribute the several hundred gallons of water used each day by every family.


History of Pipe Materials

Water has always been a precious commodity, and its transmission has facilitated the advancement civilization enabled the comforts of our modern living standard.

While the Romans were acclaimed for their transmission of water, their aqueducts provided only downhill passage, by gravity flow. Complete distribution required pressurization in pipe. Earliest pipe materials were predominantly bored logs, with some use of lead pipe and brittle baked clay pipe.

Iron pipes were first used in the 15th century in Germany and France. The most notable installation as the Palace of Versailles built by King Louis XIV in 1664. These cast iron pipes are still in use today, over 300 years later. Gray cast iron pipe progressively became the preferred material for water.

The first iron pipe in the United States was imported from England and used by the city of Philadelphia in 1804. Early Iron in the United States was made in charcoal furnaces, which were concentrated mostly in the New Jersey area. Some of the earliest pipe foundries were also located there.

With the use of coke in blast furnaces, then cupolas, foundry growth expanded westward into Pennsylvania and Ohio, then southward toward the Birmingham area, where all the materials for iron were available. Soon, various accessories such as fittings, valves and fire hydrants joined with pipe as parts of the total industry, and were cast in many foundries.

Sanitary or soil pipe also grew into a considerable industry, but distinct from pressure pipe with less demanding iron specifications, shorter lengths and thinner walls.

Since 1913, Alabama has been the leading state, and Birmingham the leading city, for iron pipe production.     back to top

Evolution of Casting Methods

The first iron pipes were cast statically in horizontal modules in lengths limited to three to six feet because of suspension of the massive center cores. Many of the early foundries produced pipe along with many other types of casting. As demand for pipe increased, the casting equipment became more specialized, casting vertically in pits with lengths increased first to 12 feet, then 16 feet.

In 1918, a Brazilian, DeLavaud, presented a centrifugal casting process which revolutionized pipe production. The use of the centrifugal force of a rotating mold eliminated need for the center core. And the water-cooled metal mold permitted repetitive casting at high production rates. Long heat treating ovens were necessary to anneal some chill obtained against the metal mold.

A centrifugal process using sand rammed molds was developed to avoid the chilled structure and necessity for annealing. Later, a resin bonded thin sand process was invented by ACIPCO and used by a few plants for several years.

With increase labor cost and the advent of Ductile Iron, which required annealing on all processes, sand lined processes have been abandoned. All pressure pipe is now cast in water cooled metal molds using highly specialized equipment with automation and computerized controls.

Gray Iron Pipe Quality Advances

With advances in metallurgy and melting controls, and through the use of chemical, and spectrometer laboratories, gray iron pipe progressively improved and its strength increased. Quality was closely controlled to specified levels of strength, and the moduli of rupture and modulus of elasticity determined on test specimens from the wall of the pipe. Each pipe was hydrostatically tested to 5O0 psi.

Twin 30 inch lines of Ductile Iron pipe being installed in one of our large cities to expand and improve water service.

Guided by a strong pipe association, thickness classifications were established for various operating pressures and depths of cover with allowances for pressure surges from valve closing and from super imposed truck loads.     back to top

Ductile Iron Evaluated and Adopted

When the discovery of Ductile Iron was announced, some pipe producers saw no need for it, since gray iron had served well and was stronger that other competitive pipe materials, primarily plastic in small diameters and reinforced concrete in large diameters. But others recognized the potential for Ductile Iron in pressure pipe service. Several companies experimented with Ductile Iron, and some trial orders were produced for special applications and evaluation. Performance tests and experiences were very favorable.

Again, the pipe association guided evaluation of Ductile Iron on test pipe of various thicknesses, outfitted with strain gages, installed in various type trenches and depths of cover and subjected to various pressures and external loads simulating passage of trucks.

These tests verified the superior properties of Ductile Iron, which permitted reduction in thickness. The established thickness reductions more than compensated for the increased cost of Ductile Iron and actually reduced the pipe cost per foot.

Through a period of transition, most companies produced both gray iron and Ductile Iron pipe to suit customer preference. But with good experience from Ductile Pipe in service, preference for Ductile Iron progressively increased. In the mid seventies, all major producers went totally to Ductile Iron and abandoned gray iron pipe. Those producers who resisted Ductile Iron were eventually closed or purchased.

Processes and Properties

With conversion to Ductile Iron, pressure pipe production became an even more specialized process.

Pipe producers generally melt in large water-cooled cupolas with the latest accessory equipment. Some producers duplex in electric furnaces for more positive supply and control. In the early years, some used a basic slag to obtain low sulfur from the cupola. In recent years, general practice has been to melt with an acid to neutral slag and desulfurize externally using on of several available agitation methods. Low sulfur iron is then treated with magnesium by several of the available treatment processes.

Magnesium treated iron with closely controlled chemistry and temperature is poured at a controlled rate into molds rotation at proper centrifugal speed with post inoculant added in the stream and mold.     back to top

After stripping, the pipes are fully annealed through long annealing furnaces, some as long as 240 feet. As-cast pipe has a slight depth of chilled iron which requires some time in a 1700°F zone. Due to the late post inoculation, the carbides break down fast to fine nodular graphite with a high nodule count. Then a lower temperature zone breaks down pearlite to a ferritic matrix for highest ductility and impact toughness.

Guided by tests the pipe association, specifications established by A.N.S.I. and A.W.W.A require tensile tests from the wall of the pipe to meet 60,000 psi tensile, 42,000 psi yield, and 10 percent elongation. Impact strength is specified both at room temperature and at -40°F on a modified Charpy-V specimen testing the full wall of the pipe.

Conclusion

The pressure pipe industry has taken advantage of the superior properties of Ductile Iron, totally converting all iron pipe to Ductile Iron.

Ductile Iron pipe has established an outstanding performance record against increasing stresses, superimposed loads and earthquakes. Ductile Iron has also enhanced the reliability of water transmission, thereby providing comfort and sanitation and contributing to our high standard of living.

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