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Deep
Cryogenic Tempering - |
An abstract of a presentation given at
the DIS Ft. Worth meetingby:
John Koucky, 300 Below, Inc.What is Deep Cryogenic Tempering?
It is -
Freezing the material at -300oF to modify the microstructure and improve the properties.
A "dry" process.
A "one time" treatment.
A "through" treatment.
A treatment to improve properties - particularly the wear properties.
What are the benefits of Deep Cryogenic Tempering?
Deep Cryogenic Treatment at -300oF can make a major contribution to solving these problems:
HIGH ABRASIVE WEAR in cutting tools, molds, dies, bearings, etc.
HIGH CORROSIVE WEAR in chemical, food and oil equipment applications.
HIGH EROSIVE WEAR from wind, water and other abrasive grit carriers.
DISTORTIONS induced by design, forming, machining or environment.
STRESS RELIEF in complex tools, components and welds.
STRESS RELIEF CRACKING in weld zones in corrosive atmospheres.
SURFACE FINISH in any applications where long life is needed.
STABILIZATION in parts and components as a result of stresses.
MACHINABILITY in aluminum and copper parts.
ELECTRODE LIFE in copper resistance welding electrodes.
What happens during Deep Cryogenic Tempering? (Ferrous components)
Most of the retained austenite is transformed into martensite. The martensite is then tempered to change it into tempered martensite.
Small complex carbides called eta carbides are precipitated out.
Residual stresses are greatly reduced.
Alloys with greater than 0.40% carbon REQUIRE Cryogenic Tempering to finish martensite transformation.
Deep Cryogenic Tempering is performed in batch type Cryo Processors using primarily liquid nitrogen. The tempering process is fully automated with computer controls to offer maximum benefits.
What materials are favorably affected by Deep Cryogenic Tempering?
Ferrous Materials:
1. Tool steels
2. Higher carbon, higher alloy materials
3. Martensitic stainless steels
4. Gray cast iron
Aluminum
Brass
Tungsten carbide
Other applications of the process are
1. Musical instruments
2. Motor sport applications
3. Gun barrels
4. Sporting goods
5. Disc brake rotors
6. Others such as composites, etc.
Deep Cryogenic Tempering at -300oF vastly improves the wear properties compared to 'cold treatment' at -100oF. (See table 1.)
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TABLE 1. Test Results (% Wear Increase after Cryogenic Tempering) |
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| Type of Steel | % Improvement | ||
|
AISI # |
Description | (-110oF) | (-310oF) |
|
D-2 |
High carbon/chromium die |
316 |
817 |
|
A-2 |
Chromium cold work die |
204 |
560 |
|
S-7 |
Silicon tool steel |
241 |
503 |
|
52100 |
Bearing steel |
195 |
420 |
|
0-1 |
Oil hardening cold work die |
221 |
418 |
|
A-10 |
Graphite tool steel |
230 |
264 |
|
M-1 |
Molybdenum high speed |
145 |
225 |
|
H-13 |
Chromium/moly hot die |
164 |
209 |
|
M-2 |
Tungsten/moly high speed |
117 |
203 |
|
T-1 |
Tungsten high speed |
141 |
176 |
|
CPM-10V |
Alloy steel |
94 |
131 |
|
P-20 |
Mold steel |
123 |
130 |
|
440 |
Martensitic stainless |
128 |
121 |
|
430 |
Ferritic stainless |
116 |
119 |
|
303 |
Austenitic stainless |
105 |
110 |
|
8620 |
Nickel-chromium-moly steel |
112 |
104 |
|
C1020 |
Carbon steel |
97 |
98 |
|
AQS |
Graphitic cast iron |
96 |
97 |
|
A-6 |
Manganese, air, cold work die |
73 |
97 |
|
T-2 |
Tungsten high speed steel |
72 |
92 |
Field test results with Deep Cryogenic Tempering. (See table 2.)
Our expert computer-controlled patented systems
which enable
CONSISTENCY AND MAXIMIZED GAIN in the following areas:
Reduced: Abrasive Wear, Corrosive Wear, Erosive Wear, Distortion
Increased: Stress Relief, Stabilization, Machinability
Significantly Increased: Useful Life
| Table 2 | |||
| Tool Type | Company | Tool Material | % Improvement |
| Drills | Aircraft Manufacturer | M42, M7, C2 | 300 |
| Milling | Aircraft Manufacturer | M7 | 250 |
| Deburring | University Study | Inconel | 400 |
| Gear Cutter | Major Manufacturer | Ti-N Coated | 350 |
| Broach | Metal Milling Co. | Carbide | 300 |
| Punching | Major Manufacturer | M7 | 600 |
| End Mill | Aerospace Mfg. | M42 | 450 |
| Hob | Turbine Mfg. | M2-M7 | 300 |
| Face Mill | Aerospace | C2 Carbide | 400 |
| Key Cutter | Aircraft Mfg. | M2-M7 | 250 |
| Slicer | Plastics Mfg. | M7 | 600 |
| Chipper | Box Mfg. | Carbide | 500 |
| Shredder | Paper Mfg. | M7 | 400 |
| Tap | Tool Maker | C2 Carbide | 600 |
| Die | Casting Company | Hi Ni Alloy | 300 |
| Dentistry | Dentist | 400 Stainless | 500 |
| Broach | Auto Mfg. | Hi Nickel | 250 |
| Logging | Logging Company | Saw Chain | 400 |
| Milling | Machine Shop | 347 Stainless | 375 |
| Woodcutting | Pro Woodworker | HSS | 500 |
| Stamping Die | Steel Furniture | D2 | 1000 |
| Corrosion | University Study | S2, M2, 4142, 316 | Red. All Corrosion |
| Machinability | Machine Shop | Thin Wall Alum. | 50% Time Savings |
| Electrode | 7 Studies | Welding | 600% Average |
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